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Structure & Reactivity II: Purification and Spectroscopy

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Structure & Reactivity II: Purification and Spectroscopy

Chem 201-203: Infrared, NMR, Mass Spectrometry, Laboratory Techniques

General ChemistryChemistry
Author
Chris Schaller
Publisher
College of Saint Benedict/Saint John's University
Source
LibreTexts
License
CC BY-NC
Language
EN
Category
Basic Sciences
Read online Download PDF (open licence)
Contents· 79 sections
  1. 01: Introduction to Spectoscopy
  2. 02: Ultraviolet-Visible Spectroscopy
  3. 2.01: Introduction to UV Spectroscopy
  4. 2.02: UV-Visible Spectroscopy - Metal Ions
  5. 2.03: UV-Visible Spectroscopy of Organic Compounds
  6. 2.04: UV-Visible Spectroscopy- Solutions.
  7. 03: Infrared Spectroscopy
  8. 3.01: Introduction
  9. 3.02: Hydrocarbon Spectra
  10. 3.03: Some Subtle Points of IR Spectroscopy
  11. 3.04: Carbon-Carbon Multiple Bonds
  12. 3.05: Bonds to Common Heteroatoms- Oxygen
  13. 3.06: Carbon-Oxygen Double Bonds
  14. 3.07: Bonds to Common Heteroatoms- Nitrogen
  15. 3.08: More Complicated Spectra
  16. 3.09: Misleading Peaks
  17. 3.10: Additional Problems
  18. 3.11: Solutions for Selected Problems
  19. 3.12: Appendix
  20. 04: Nuclear Magnetic Resonance Spectroscopy
  21. 4.01: Introduction
  22. 4.02: C NMR Spectroscopy
  23. 4.03: Symmetry in Spectroscopy
  24. 4.04: Factors in Chemical Shift- Carbon Geometry
  25. 4.05: Factors in Chemical Shift- Electronegativity
  26. 4.06: More on Electronic Effects
  27. 4.07: H NMR Spectroscopy
  28. 4.08: Chemical Shift in Proton Spectra
  29. 4.09: Integration
  30. 4.10: Multiplicity
  31. 4.11: More Complicated Coupling
  32. 4.12: Constructing Partial Structures in NMR Spectroscopy and Combined Structure Determination
  33. 4.13: NMR in Lab- Solvent Impurities
  34. 4.14: NMR in Lab- Monitoring Reaction Progress
  35. 4.15: NMR in Lab- Composition of Mixtures
  36. 4.16: More Practice
  37. 4.17: 2D NMR
  38. 4.18: Solutions to Selected Problems
  39. 4.19: Appendix
  40. 05: 2D NMR
  41. 5.01: COSY Spectra
  42. 5.02: TOCSY Spectra
  43. 5.03: HMBC and HMQC Spectra
  44. 5.04: NOESY Spectra
  45. 5.05: Proteins
  46. 5.06: More Practice with 2D
  47. 5.07: 2D NMR Solutions
  48. 06: Introductory Mass Spectrometry
  49. 6.01: Introduction to Mass Spectrometry
  50. 6.02: The Mass Spectrometry Experiment
  51. 6.03: GC-MS and LC-MS
  52. 6.04: Molecular Ions
  53. 6.05: Molecular Weight Molecular Formula and Degrees of Unsaturation
  54. 6.06: Isotopomers
  55. 6.07: Other Important Isotopes- Br and Cl
  56. 6.08: Molecular Weight- Even or Odd
  57. 6.09: High vs Low Resolution
  58. 6.10: Fragmentation - Stable Cations
  59. 6.11: Fragmentation Pathways
  60. 6.12: Solutions for Selected Problems
  61. 07: Purification of Molecular Compounds
  62. 7.01: Evaporation
  63. 7.02: Filtration
  64. 7.03: Distillation
  65. 7.04: Sublimation
  66. 7.05: Recrystallization
  67. 7.06: Solvent Partitioning (Liquid-Liquid Extraction)
  68. 7.07: Acid-Base Extraction
  69. 7.08: Liquid Chromatography
  70. 7.09: Column Chromatography (Normal Phase)
  71. 7.10: Reverse Phase Chromatography
  72. 7.11: Size Exclusion Chromatography
  73. 7.12: Ion Exchange Chromatography
  74. 7.13: Affinity Chromatography
  75. 7.14: Electrophoresis
  76. 7.15: Instrumentation Using Chromatography
  77. 7.16: Solutions for Selected Problems
  78. 08: Lab Basics
  79. 8.01: Dissolution