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Analytical Chemistry 2.0

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Analytical Chemistry 2.0

Analytical chemistry spans nearly all areas of chemistry but involves the development of tools and methods to measure physical properties of substances and apply those techniques to the identification of their presence (qualitative analysis) and quantify the amount present (quantitative analysis) of species in a wide variety of settings.

Chemistry
Author
David Harvey
Publisher
DePauw University
Source
LibreTexts
License
CC BY-NC-SA
Language
EN
Category
Basic Sciences
Read online Download PDF (open licence)
Contents· 141 sections
  1. 01: Front Matter
  2. 1.1: TitlePage
  3. 1.2: InfoPage
  4. 1.3: Table of Contents
  5. 02: Introduction to Analytical Chemistry
  6. 2.1: What is Analytical Chemistry?
  7. 2.2: The Analytical Perspective
  8. 2.3: Common Analytical Problems
  9. 2.4: Introduction to Analytical Chemistry (Exercises)
  10. 2.5: Introduction to Analytical Chemistry (Summary)
  11. 03: Basic Tools of Analytical Chemistry
  12. 3.1: Measurements in Analytical Chemistry
  13. 3.2: Concentration
  14. 3.3: Stoichiometric Calculations
  15. 3.4: Basic Equipment
  16. 3.5: Preparing Solutions
  17. 3.6: Spreadsheets and Computational Software
  18. 3.7: The Laboratory Notebook
  19. 3.8: Basic Tools of Analytical Chemistry (Exercises)
  20. 3.9: Basic Tools of Analytical Chemistry (Summary)
  21. 04: The Vocabulary of Analytical Chemistry
  22. 4.1: Analysis, Determination, and Measurement
  23. 4.2: Techniques, Methods, Procedures, and Protocols
  24. 4.3: Classifying Analytical Techniques
  25. 4.4: Selecting an Analytical Method
  26. 4.5: Developing the Procedure
  27. 4.6: Protocols
  28. 4.7: The Importance of Analytical Methodology
  29. 4.8: The Vocabulary of Analytical Chemistry (Exercises)
  30. 4.9: The Vocabulary of Analytical Chemistry (Summary)
  31. 05: Evaluating Analytical Data
  32. 5.01: Characterizing Measurements and Results
  33. 5.02: Characterizing Experimental Errors
  34. 5.03: Propagation of Uncertainty
  35. 5.04: The Distribution of Measurements and Results
  36. 5.05: Statistical Analysis of Data
  37. 5.06: Statistical Methods for Normal Distributions
  38. 5.07: Detection Limits
  39. 5.08: Using Excel and R to Analyze Data
  40. 5.09: Evaluating Analytical Data (Exercises)
  41. 5.10: Evaluating Analytical Data (Summary)
  42. 06: Standardizing Analytical Methods
  43. 6.1: Analytical Standards
  44. 6.2: Calibrating the Signal
  45. 6.3: Determining the Sensitivity
  46. 6.4: Linear Regression and Calibration Curves
  47. 6.5: Blank Corrections
  48. 6.6: Using Excel and R for a Regression Analysis
  49. 6.7: Standardizing Analytical Methods (Exercises)
  50. 6.8: Standardizing Analytical Methods (Summary)
  51. 07: Equilibrium Chemistry
  52. 7.01: Reversible Reactions and Chemical Equilibria
  53. 7.02: Thermodynamics and Equilibrium Chemistry
  54. 7.03: Manipulating Equilibrium Constants
  55. 7.04: Equilibrium Constants for Chemical Reactions
  56. 7.05: Le Châtelier’s Principle
  57. 7.06: Ladder Diagrams
  58. 7.07: Solving Equilibrium Problems
  59. 7.08: Buffer Solutions
  60. 7.09: Activity Effects
  61. 7.10: Using Excel and R to Solve Equilibrium Problems
  62. 7.11: Some Final Thoughts on Equilibrium Calculations
  63. 7.12: Equilibrium Chemistry (Exercises)
  64. 7.13: Equilibrium Chemistry (Summary)
  65. 08: Collecting and Preparing Samples
  66. 8.01: The Importance of Sampling
  67. 8.02: Designing a Sampling Plan
  68. 8.03: Implementing the Sampling Plan
  69. 8.04: Separating the Analyte from Interferents
  70. 8.05: General Theory of Separation Efficiency
  71. 8.06: Classifying Separation Techniques
  72. 8.07: Liquid–Liquid Extractions
  73. 8.08: Separation Versus Preconcentration
  74. 8.09: Collecting and Preparing Samples (Exercises)
  75. 8.10: Collecting and Preparing Samples (Summary)
  76. 09: Gravimetric Methods
  77. 9.1: Overview of Gravimetric Methods
  78. 9.2: Precipitation Gravimetry
  79. 9.3: Volatilization Gravimetry
  80. 9.4: Particulate Gravimetry
  81. 9.5: Gravimetric Methods (Exercises)
  82. 9.6: Gravimetric Methods (Summary)
  83. 10: Titrimetric Methods
  84. 10.1: Overview of Titrimetry
  85. 10.2: Acid–Base Titrations
  86. 10.3: Complexation Titrations
  87. 10.4: Redox Titrations
  88. 10.5: Precipitation Titrations
  89. 10.6: Titrimetric Methods (Exercises)
  90. 10.7: Titrimetric Methods (Summary)
  91. 11: Spectroscopic Methods
  92. 11.01: Overview of Spectroscopy
  93. 11.02: Spectroscopy Based on Absorption
  94. 11.03: UV
  95. Vis and IR Spectroscopy
  96. 11.04: Atomic Absorption Spectroscopy
  97. 11.05: Emission Spectroscopy
  98. 11.06: Photoluminescence Spectroscopy
  99. 11.07: Atomic Emission Spectroscopy
  100. 11.08: Spectroscopy Based on Scattering
  101. 11.09: Spectroscopic Methods (Exercises)
  102. 11.10: Spectroscopic Methods (Summary)
  103. 12: Electrochemical Methods
  104. 12.1: Overview of Electrochemistry
  105. 12.2: Potentiometric Methods
  106. 12.3: Coulometric Methods
  107. 12.4: Voltammetric Methods
  108. 12.5: Electrochemical Methods (Exercises)
  109. 12.6: Electrochemical Methods (Summary)
  110. 13: Chromatographic
  111. 13.1: Overview of Analytical Separations
  112. 13.2: General Theory of Column Chromatography
  113. 13.3: Optimizing Chromatographic Separations
  114. 13.4: Gas Chromatography
  115. 13.5: High-Performance Liquid Chromatography
  116. 13.6: Other Forms of Liquid Chromatography
  117. 13.7: Electrophoresis
  118. 13.8: Chromatographic and Electrophoretic Methods (Exercises)
  119. 13.9: Chromatographic and Electrophoretic Methods (Summary)
  120. 14: Kinetic Methods
  121. 14.1: Kinetic Methods Versus Equilibrium Methods
  122. 14.2: Chemical Kinetics
  123. 14.3: Radiochemistry
  124. 14.4: Flow Injection Analysis
  125. 14.5: Kinetic Methods (Exercises)
  126. 14.6: Kinetic Methods (Summary)
  127. 15: Developing a Standard Method
  128. 15.1: Optimizing the Experimental Procedure
  129. 15.2: Verifying the Method
  130. 15.3: Validating the Method as a Standard Method
  131. 15.4: Using Excel and R for an Analysis of Variance
  132. 15.5: Developing a Standard Method (Exercises)
  133. 15.6: Developing a Standard Method (Summary)
  134. 16: Quality Assurance
  135. 16.1: The Analytical Perspective—Revisited
  136. 16.2: Quality Control
  137. 16.3: Quality Assessment
  138. 16.4: Evaluating Quality Assurance Data
  139. 16.5: Quality Assurance (Exercises)
  140. 17: Additional Resources
  141. 18: Back Matter