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UIS: Introduction to Organic Spectroscopy

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UIS: Introduction to Organic Spectroscopy

Chemistry
Publisher
University of Illinois, Springfield
Source
LibreTexts
License
CC BY-NC-SA
Language
EN
Category
Basic Sciences
Read online Download PDF (open licence)
Contents· 138 sections
  1. 1: Introduction to Organic Spectroscopy
  2. 1.1: 12.0 Introduction
  3. 1.2: 12.5 Spectroscopy and the Electromagnetic Spectrum
  4. 1.3: Electromagnetic Radiation
  5. 1.4: Introduction to Spectroscopy
  6. 1.5: The Power of the Fourier Transform for Spectroscopists
  7. 1.6: Time-resolved vs. Frequency Resolved
  8. 2: Mass Spectrometry
  9. 2.1: Introduction to Mass Spectrometry
  10. 2.2: Mass Spectrometry
  11. 2.3: How the Mass Spectrometer Works
  12. Electrospray Ionization Mass Spectrometry
  13. Injection Stage
  14. MALDI-TOF
  15. Mass Analyzers (Mass Spectrometry)
  16. 2.4: Interpretation of Mass Spectra
  17. 13C
  18. Br and Cl
  19. Fragmentation
  20. Fragmentation Patterns in Mass Spectra
  21. Molecular Ion and Nitrogen
  22. Molecular Ions
  23. Organic Compounds Containing Halogen Atoms
  24. The M 1 Peak
  25. The Molecular Ion (M) Peak
  26. 2.5: Mass Spectrometry Problems
  27. LEGO Exercise
  28. 2.6: ESI-QTOF-MS Coupled to HPLC and its Application for Food Safety
  29. 3: Infrared Spectroscopy
  30. 3.01: Infrared Spectroscopy
  31. 3.02: IR Spectroscopy
  32. 3.03: Theory
  33. How an FTIR Spectrometer Operates
  34. Theory
  35. 3.04: ATR-FTIR
  36. 3.05: Instrumentation
  37. 3.06: Sample Handling
  38. 3.07: Interpreting Infrared Spectra
  39. 3.08: Interpreting Infrared Spectra
  40. Carbon Nitrogen Bonds
  41. IR Table of Organic Compounds
  42. IR2. Hydrocarbon Spectra
  43. IR3. Subtle Points of IR Spectroscopy
  44. IR4. Carbon Carbon Multiple Bonds
  45. IR5. Carbon Oxygen Single Bonds
  46. IR6. Carbon Oxygen Double Bonds
  47. IR8. More Complicated IR Spectra
  48. IR9. Misleading Peaks
  49. IR10. More Practice with IR Spectra
  50. What Does an IR Spectrum Look Like
  51. 3.09: Interpretation
  52. 3.10: Identifying the Presence of Particular Groups
  53. 3.11: Infrared Spectra of Some Common Functional Groups
  54. 3.12: Application
  55. 4: Conjugated Compounds and Ultraviolet Spectroscopy
  56. 4.01: Chapter Objectives
  57. 4.02: 14.0 Introduction
  58. 4.03: Molecular Orbital Theory
  59. 4.04: Allylic Carbocations
  60. 4.05: 14.3 Kinetic vs. Thermodynamic Control of Reactions
  61. 4.06: 14.4 The Diels-Alder Cycloaddition Reaction
  62. 4.07: 14.5 Characteristics of the Diels-Alder Reaction
  63. 4.08: Natural and Synthetic Rubbers
  64. 4.09: Ultraviolet Spectroscopy
  65. 4.10: The Effect of Conjugation
  66. 4.11: 14.9 Conjugation Color and the Chemistry of Vision
  67. 4.12: UV-Visible Spectroscopy
  68. 5: Proton Nuclear Magnetic Resonance Spectroscopy (NMR)
  69. 5.01: Nuclear Magnetic Resonance Spectroscopy
  70. 5.02: Introduction
  71. 5.03: NMR Spectroscopy
  72. 5.04: Theory
  73. Bloch Equations
  74. Larmor Precession
  75. NMR Interactions
  76. Quantum Mechanic Treatment
  77. Relaxation
  78. Rotations and Irreducible Tensor Operators
  79. 5.05: The Nature of NMR Absorptions
  80. 5.06: Interpretation
  81. 5.07: Interpretation
  82. Integration in NMR
  83. Pascals Triangle
  84. 5.08: Structural Assignment
  85. (n 1) Rule
  86. Background to C-13 NMR
  87. Determine Structure with Combined Spectra
  88. High Resolution Proton NMR Spectra
  89. Integration in Proton NMR
  90. Interpreting C-13 NMR Spectra
  91. Introduction to Proton NMR
  92. Low Resolution Proton NMR Spectra
  93. More About Electronics
  94. Multiplicity in Proton NMR
  95. NMR Appendix. Useful Charts for NMR identification
  96. NMR2. Carbon-13 NMR
  97. NMR3. Symmetry in NMR
  98. NMR4. 13C NMR and Geometry
  99. NMR5. 13C NMR and Electronics
  100. NMR8. Chemical Shift in 1H NMR
  101. NMR11. More About Multiplicity
  102. NMR14. More Practice with NMR Spectroscopy
  103. 5.09: Active Learning with NMR
  104. In-Class Questions
  105. Set 1 Basic Concepts
  106. Set 2 Energy Transition and Population
  107. Set 3 Electron Shielding
  108. Set 4 Nuclear Coupling
  109. Set 5 Exchange Effects
  110. Set 6 Classical Description
  111. Instructors Manual
  112. Learning Objectives
  113. Text
  114. 5.10: Chemical Shifts
  115. 5.11: (1H) NMR Spectroscopy and Proton Equivalence
  116. 5.12: Chemical Shifts in (1H) NMR Spectroscopy
  117. 5.13: Integration of Proton Spectra
  118. 5.14: Spin-Spin Splitting in (1H) NMR Spectra
  119. 5.15: Chemical Equivalence
  120. 5.16: More Complex Spin-Spin Splitting Patterns
  121. 5.17: Uses of (1H) NMR Spectroscopy
  122. 6: Carbon-13 NMR Spectroscopy
  123. 6.1: Interpreting C-13 NMR Spectra
  124. 13.4 (13C) NMR Spectroscopy: Signal Averaging and FT-NMR
  125. 13.5 Characteristics of (13C) NMR Spectroscopy
  126. 13.7 Uses of (13C) NMR Spectroscopy
  127. 7: Two-Dimensional NMR Spectroscopy
  128. 7.1: 2D NMR
  129. 2D NMR Background
  130. 2D NMR Basics
  131. 2D NMR Experiments
  132. 2D NMR Introduction
  133. Heteronuclear Correlations
  134. Homonuclear Correlations
  135. Indirect Detection
  136. 7.2 J-Resolved
  137. 13.6: DEPT C NMR Spectroscopy
  138. 8: Multinuclear Magnetic Resonance Spectroscopy