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Lab Manual: Analytical Chemistry at Duke

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Lab Manual: Analytical Chemistry at Duke

Lab manual for Analytical Chemistry Lab (CHEM401L) at Duke University.

Chemistry
Author
Kathryn Haas
Publisher
Duke University
Source
LibreTexts
License
CC BY-NC-SA
Language
EN
Category
Basic Sciences
Read online Download PDF (open licence)
Contents· 52 sections
  1. 01: Orientation to this course
  2. 1.01: Pre-lab orientation assignment
  3. 1.02: Introductory Details
  4. 1.03: Grading and Rubrics
  5. 1.04: Statements
  6. 02: Calibration and Quantitative Techniques
  7. 2.01: Procedure and instructions for data analysis
  8. 2.02: Analytical Lab Equiptment
  9. 2.03: Preparing Solutions
  10. 2.04: Operating Instructions for Spec 20's
  11. 2.05: Uncertainty in values determined from a Calibration Curve
  12. 2.06: Methods of Calibration
  13. 2.07: (old) Pre-lab assignment
  14. 03: Determining caffeine in beverages using HPLC (and UV-vis)
  15. 3.01: HPLC and UV-vis Prelab Assignment
  16. 3.02: Pre-Lab Assigment
  17. 3.03: Introduction to UV-vis and HPLC
  18. 3.3.01: Absorbance and Beer's Law
  19. 3.3.02: UV Vis Instrumentation
  20. 3.3.03: High performance liquid chromatography
  21. 3.3.04: HPLC Instruments at Duke
  22. 3.04: UV-vis procedure and instructions for data analysis
  23. 3.05: HPLC procedure and instructions for data analysis
  24. 3.5.01: Writing a Method for the Agilent 1100 1200 HPLC
  25. 3.5.02: Set up a sequence for the Agilent 1100 1200 HPLC
  26. 3.5.03: Running a Sequence
  27. 3.06: TA Notes
  28. 04: Determination of cocaine on bills using Gas Chromatography Mass Spectrometry (GC-MS)
  29. 4.01: GC-MS Pre-Lab Assignment
  30. 4.02: Introduction to Gas Chromatography Instrumentation
  31. 4.03: Quantitative and Qualitative GC and GC-MS
  32. 4.04: Mass Spectrometers
  33. 4.05: Interpreting Electron Ionization Mass Spectra
  34. 4.06: GC-MS Procedure and instructions for data analysis
  35. 4.07: GC-MS Instruments at Duke
  36. 4.08: Instructions for Operating the Agilent 7820A 5975 GCMS (Autosampler)
  37. 4.09: Data Analysis with Agilent Mass Hunter Qualitative Software
  38. 4.10: Data Analysis using Agilent Mass Hunter Quantitative Analysis
  39. 4.11: TA Notes
  40. 4.12: Archive of GCMS procedure
  41. 4.12.01: Instructions for Data Processing using MSD ChemStation Data Analysis Software
  42. 4.12.02: Instructions for Operating the Agilent 7820A 5975 GCMS (Manual)
  43. 4.12.03: Archived GC-MS Pre-Lab Assignment (Fall 2024)
  44. 05: Determination of metals using Inductively coupled plasma optical emission spectroscopy (ICP-OES)
  45. 5.01: Pre-Lab assignment
  46. 5.02: Atomic Emission Spectroscopy
  47. 5.03: ICP-OES Procedure and instructions for treatment of data
  48. 5.04: ICP-OES Instrument at Duke
  49. 5.05: Writing a method for the Perkin Elmer Avio 220 Max
  50. 5.06: ICP-OES Operation Instructions
  51. 5.07: Instructions for Viewing and Exporting Data using Syngistics Software
  52. 5.08: TA Notes