Nguồn ngoài
The Schlenk Line Survival Guide
The text is a practical resource designed to help chemists working with air-sensitive compounds. It provides step-by-step guides on using a Schlenk line, a common lab apparatus for handling compounds under an inert atmosphere like nitrogen or argon. The guide covers essential techniques, including how to properly set up and operate the Schlenk line, perform Schlenk transfers, and filter solutions under an inert atmosphere. It also emphasizes safety procedures and troubleshooting common issues.
- Tác giả
- Andryj Borys
- Nhà xuất bản
- Universität Bern
- Nguồn
- LibreTexts
- Giấy phép
- CC BY-NC
- Ngôn ngữ
- EN
- Danh mục
- Khoa học cơ bản
Mục lục· 22 mục
- 01: Guides
- 1.01: The Schlenk Line
- 1.02: Cycling onto the Schlenk Line
- 1.03: Performing Sensitive Reactions without a Schlenk Line
- 1.04: Transferring Liquids
- 1.4.01: Cannula Transfer
- 1.4.02: Syringes and Sure Seals
- 1.05: Inert Atmosphere Filtrations
- 1.5.01: Cannula Filtration
- 1.5.02: Filtration through Celite
- 1.06: NMR Preparation
- 1.6.01: Preparing NMR Samples on a Schlenk Line
- 1.6.02: Removing Solvent from NMR tubes
- 1.07: Distillations
- 1.7.01: Static Vacuum Distillation
- 1.7.02: Dynamic Vacuum Distillation
- 1.08: Freeze-Pump-Thaw
- 1.09: Drying Solvents
- 1.10: Removing Solvent
- 1.11: Addition of Solids
- 1.12: Refluxing Under an Inert Atmosphere
- 1.13: Gloveboxes